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Preparation and characterization of multiwalled carbon nanotube/In2O3 composites

Identifieur interne : 000673 ( Main/Repository ); précédent : 000672; suivant : 000674

Preparation and characterization of multiwalled carbon nanotube/In2O3 composites

Auteurs : RBID : Pascal:13-0323805

Descripteurs français

Pascal (Inist)
- Préparation, Caractérisation, Nanotube multifeuillet, Nanotube multifeuillets, Nanotube carbone, Oxyde d'indium, Matériau composite, 8107D, In2O3.
Wicri :
- concept : Matériau composite.

English descriptors

KwdEn :
- Carbon nanotubes, Characterization, Composite materials, Indium oxide, Multiwalled nanotube, Preparation.

Abstract

We have prepared multiwalled carbon nanotube (MWCNT)/In₂O₃ composites using a simple impregnation method. The precursor compound indium(III) chloride (InCl₃) was used to cover the surface of MWCNTs and distilled water was used as solvent. The applied mass ratio was 4:1 (In₂O₃/MWCNT), and during the calcination process different temperatures (300, 350 and 400 °C) were investigated. The produced materials were characterized by X-ray diffraction, energy-dispersive X-ray spectroscopy, Raman spectroscopy, Fourier transform infrared spectroscopy, transmission and scanning electron microscopy, and a thermogravimetric analysis was executed also. The average thickness of the produced surface layer and the average sizes of the In₂O₃ particles were calculated with the Scherrer formula and the ImageJ-program. The results show that the heat treatment temperature affected the characteristic morphology and the crystal structure of the as-prepared composite. These multiwalled carbon nanotube-based composites are promising candidates as gas sensors and catalyst.

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Pascal:13-0323805

Le document en format XML

<record><TEI><teiHeader><fileDesc><titleStmt><title xml:lang="en" level="a">Preparation and characterization of multiwalled carbon nanotube/In<sub>2</sub>
O<sub>3</sub>
 composites</title>
<author><name sortKey="Berki, Peter" uniqKey="Berki P">Peter Berki</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Department of Applied and Environmental Chemistry, University of Szeged, Rerrich B. tér 1</s1>
<s2>Szeged 6720</s2>
<s3>HUN</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>8 aut.</sZ>
</inist:fA14>
<country>Hongrie</country>
<wicri:noRegion>Szeged 6720</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Nemeth, Zolt N" uniqKey="Nemeth Z">Zolt N Nemeth</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Department of Applied and Environmental Chemistry, University of Szeged, Rerrich B. tér 1</s1>
<s2>Szeged 6720</s2>
<s3>HUN</s3>
<sZ>1 aut.</sZ>
<sZ>2 aut.</sZ>
<sZ>3 aut.</sZ>
<sZ>8 aut.</sZ>
</inist:fA14>
<country>Hongrie</country>
<wicri:noRegion>Szeged 6720</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Reti, Bal Zs" uniqKey="Reti B">Bal Zs Reti</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Department of Applied and Environmental Chemistry, University of Szeged, Rerrich B. tér 1</s1>
<s2>Szeged 6720</s2>
<s3>HUN</s3>
<sZ>1 aut.</sZ>
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<country>Hongrie</country>
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</author>
<author><name sortKey="Berkesi, Ott" uniqKey="Berkesi O">Ott Berkesi</name>
<affiliation wicri:level="1"><inist:fA14 i1="02"><s1>Department of Physical Chemistry and Materials Science, University of Szeged, Rerrich B. tér 1</s1>
<s2>Szeged 6720</s2>
<s3>HUN</s3>
<sZ>4 aut.</sZ>
</inist:fA14>
<country>Hongrie</country>
<wicri:noRegion>Szeged 6720</wicri:noRegion>
</affiliation>
</author>
<author><name sortKey="Magrez, Arnaud" uniqKey="Magrez A">Arnaud Magrez</name>
<affiliation wicri:level="4"><inist:fA14 i1="03"><s1>Laboratory of Physics of Complex Matter, EPFL</s1>
<s2>Ecublens 1026</s2>
<s3>CHE</s3>
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<sZ>7 aut.</sZ>
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<country>Suisse</country>
<placeName><settlement type="city">Lausanne</settlement>
<region nuts="3" type="region">Canton de Vaud</region>
</placeName>
<orgName type="university">École polytechnique fédérale de Lausanne</orgName>
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</author>
<author><name sortKey="Aroutiounian, Vladimir" uniqKey="Aroutiounian V">Vladimir Aroutiounian</name>
<affiliation wicri:level="1"><inist:fA14 i1="04"><s1>Center of Semiconductor Devices and Nanotechnologies, Yerevan State University, 1 Manoukian St.</s1>
<s2>Yerevan 0025</s2>
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<country>Arménie</country>
<wicri:noRegion>Yerevan 0025</wicri:noRegion>
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<author><name sortKey="Forro, L Szl" uniqKey="Forro L">L Szl Forro</name>
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<country>Suisse</country>
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<author><name sortKey="Hernadi, Klara" uniqKey="Hernadi K">Klara Hernadi</name>
<affiliation wicri:level="1"><inist:fA14 i1="01"><s1>Department of Applied and Environmental Chemistry, University of Szeged, Rerrich B. tér 1</s1>
<s2>Szeged 6720</s2>
<s3>HUN</s3>
<sZ>1 aut.</sZ>
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<sZ>8 aut.</sZ>
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<country>Hongrie</country>
<wicri:noRegion>Szeged 6720</wicri:noRegion>
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<publicationStmt><idno type="inist">13-0323805</idno>
<date when="2013">2013</date>
<idno type="stanalyst">PASCAL 13-0323805 INIST</idno>
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<idno type="wicri:Area/Main/Corpus">000670</idno>
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<keywords scheme="Pascal" xml:lang="fr"><term>Préparation</term>
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<term>Nanotube multifeuillets</term>
<term>Nanotube carbone</term>
<term>Oxyde d'indium</term>
<term>Matériau composite</term>
<term>8107D</term>
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<front><div type="abstract" xml:lang="en">We have prepared multiwalled carbon nanotube (MWCNT)/In<sub>2</sub>
O<sub>3</sub>
 composites using a simple impregnation method. The precursor compound indium(III) chloride (InCl<sub>3</sub>
) was used to cover the surface of MWCNTs and distilled water was used as solvent. The applied mass ratio was 4:1 (In<sub>2</sub>
O<sub>3</sub>
/MWCNT), and during the calcination process different temperatures (300, 350 and 400 °C) were investigated. The produced materials were characterized by X-ray diffraction, energy-dispersive X-ray spectroscopy, Raman spectroscopy, Fourier transform infrared spectroscopy, transmission and scanning electron microscopy, and a thermogravimetric analysis was executed also. The average thickness of the produced surface layer and the average sizes of the In<sub>2</sub>
O<sub>3</sub>
 particles were calculated with the Scherrer formula and the ImageJ-program. The results show that the heat treatment temperature affected the characteristic morphology and the crystal structure of the as-prepared composite. These multiwalled carbon nanotube-based composites are promising candidates as gas sensors and catalyst.</div>
</front>
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<sZ>4 aut.</sZ>
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<s2>Ecublens 1026</s2>
<s3>CHE</s3>
<sZ>5 aut.</sZ>
<sZ>7 aut.</sZ>
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<fA14 i1="04"><s1>Center of Semiconductor Devices and Nanotechnologies, Yerevan State University, 1 Manoukian St.</s1>
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O<sub>3</sub>
 composites using a simple impregnation method. The precursor compound indium(III) chloride (InCl<sub>3</sub>
) was used to cover the surface of MWCNTs and distilled water was used as solvent. The applied mass ratio was 4:1 (In<sub>2</sub>
O<sub>3</sub>
/MWCNT), and during the calcination process different temperatures (300, 350 and 400 °C) were investigated. The produced materials were characterized by X-ray diffraction, energy-dispersive X-ray spectroscopy, Raman spectroscopy, Fourier transform infrared spectroscopy, transmission and scanning electron microscopy, and a thermogravimetric analysis was executed also. The average thickness of the produced surface layer and the average sizes of the In<sub>2</sub>
O<sub>3</sub>
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Preparation and characterization of multiwalled carbon nanotube/In2O3 composites

Preparation and characterization of multiwalled carbon nanotube/In2O3 composites

Descripteurs français

English descriptors

Abstract

Links toward previous steps (curation, corpus...)

Links to Exploration step

Le document en format XML

Pour manipuler ce document sous Unix (Dilib)

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